FUNCTIONALIZED CALIXSPHERANDS - SYNTHESIS AND PEPTIDE COUPLING

WII BAKKER, M HAAS, HJ DENHERTOG, W VERBOOM, D DEZEEUW, AP BRUINS, DN REINHOUDT

Research output: Contribution to journalArticleAcademicpeer-review

18 Citations (Scopus)

Abstract

Calixspherands, like 1, form kinetically stable complexes with alkali metal cations. For practical in vivo applications coupling of these complexes with carrier molecules is mandatory, Therefore, a general method for the synthesis of functionalized calixspherand 17 was developed starting from functionalized m-terphenyl 10 and p-tert-butylcalix[4]arene (14). The functionalized m-terphenyl was synthesized by a Suzuki-cross-coupling reaction. Functionalized calixspherand 17 has been coupled to a low molecular weight protein.

Original languageEnglish
Pages (from-to)972-976
Number of pages5
JournalJournal of Organic Chemistry
Volume59
Issue number5
Publication statusPublished - 11-Mar-1994

Keywords

  • MOLECULAR-WEIGHT PROTEINS
  • HOST GUEST COMPLEXATION
  • CALIX<4>ARENES
  • HEMISPHERANDS
  • CATIONS
  • ACID

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