High-resolution and conventional electron microscopy study of a Sigma=3, [101]{121} twin grain boundary in molybdenum

T Vystavel*, JM Penisson, A Gemperle

*Corresponding author for this work

Research output: Contribution to journalArticleAcademicpeer-review

19 Citations (Scopus)

Abstract

Complete structural analysis of a Mo bicrystal containing a Sigma =3, [101](1 (2) over bar1)(A) grain boundary (GB) was achieved by means of transmission electron microscopy from the microscopic to the nanoscopic level. Secondary GB dislocations compensating a small deviation from the exact Sigma =3 concidence were observed and their character was determined. Rigid-body displacements (RBDs) were determined directly from high-resolution electron microscopy images using samples with surface normal parallel and perpendicular to the tilt axis. Measured values of RBDs are compared with recent theoretical calculations.

Original languageEnglish
Pages (from-to)417-429
Number of pages13
JournalPhilosophical Magazine A-Physics of Condensed Matter Structure Defects and Mechanical Properties
Volume81
Issue number2
Publication statusPublished - Feb-2001

Keywords

  • TRANSITION-METALS
  • ATOMIC-STRUCTURE
  • DISLOCATIONS
  • SIMULATION
  • SCIENCE
  • FORCES
  • HREM

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