TY - JOUR
T1 - Laser powder bed fusion of 17–4 PH stainless steel
T2 - A comparative study on the effect of heat treatment on the microstructure evolution and mechanical properties
AU - Sabooni, S.
AU - Chabok, A.
AU - Feng, S. C.
AU - Blaauw, H.
AU - Pijper, T. C.
AU - Yang, H. J.
AU - Pei, Y. T.
N1 - Funding Information:
This research was carried out under project number 15808/S16044 in the framework of the Partnership Program of the Materials innovation institute M2i ( www.m2i.nl ) and the Technology Foundation STW ( www.stw.nl ), which is part of the Netherlands Organization for Scientific Research ( www.nwo.nl ). Shaochuan Feng acknowledges Beijing Natural Science Foundation ( 3214049 ) and Fundamental Research Funds for the Central Universities , China ( QNXM20210026 ) for financial support.
Publisher Copyright:
© 2021 The Authors
PY - 2021/10
Y1 - 2021/10
N2 - 17–4 PH (precipitation hardening) stainless steel is commonly used for the fabrication of complicated molds with conformal cooling channels using laser powder bed fusion process (L-PBF). However, their microstructure in the as-printed condition varies notably with the chemical composition of the feedstock powder, resulting in different age-hardening behavior. In the present investigation, 17–4 PH stainless steel components were fabricated by L-PBF from two different feedstock powders, and subsequently subjected to different combinations of post-process heat treatments. It was observed that the microstructure in as-printed conditions could be almost fully martensitic or ferritic, depending on the ratio of Creq/Nieq of the feedstock powder. Aging treatment at 480 °C improved the yield and ultimate tensile strengths of the as-printed components. However, specimens with martensitic structures exhibited accelerated age-hardening response compared with the ferritic specimens due to the higher lattice distortion and dislocation accumulation, resulting in the “dislocation pipe diffusion mechanism”. It was also found that the martensitic structures were highly susceptible to the formation of reverted austenite during direct aging treatment, where 19.5% of austenite phase appeared in the microstructure after 15 h of direct aging. Higher fractions of reverted austenite activates the transformation induced plasticity and improves the ductility of heat treated specimens. The results of the present study can be used to tailor the microstructure of the L-PBF printed 17–4 PH stainless steel by post-process heat treatments to achieve a good combination of mechanical properties.
AB - 17–4 PH (precipitation hardening) stainless steel is commonly used for the fabrication of complicated molds with conformal cooling channels using laser powder bed fusion process (L-PBF). However, their microstructure in the as-printed condition varies notably with the chemical composition of the feedstock powder, resulting in different age-hardening behavior. In the present investigation, 17–4 PH stainless steel components were fabricated by L-PBF from two different feedstock powders, and subsequently subjected to different combinations of post-process heat treatments. It was observed that the microstructure in as-printed conditions could be almost fully martensitic or ferritic, depending on the ratio of Creq/Nieq of the feedstock powder. Aging treatment at 480 °C improved the yield and ultimate tensile strengths of the as-printed components. However, specimens with martensitic structures exhibited accelerated age-hardening response compared with the ferritic specimens due to the higher lattice distortion and dislocation accumulation, resulting in the “dislocation pipe diffusion mechanism”. It was also found that the martensitic structures were highly susceptible to the formation of reverted austenite during direct aging treatment, where 19.5% of austenite phase appeared in the microstructure after 15 h of direct aging. Higher fractions of reverted austenite activates the transformation induced plasticity and improves the ductility of heat treated specimens. The results of the present study can be used to tailor the microstructure of the L-PBF printed 17–4 PH stainless steel by post-process heat treatments to achieve a good combination of mechanical properties.
KW - 17-4 PH stainless steel
KW - Age hardening
KW - Laser powder bed fusion
KW - Post-process heat treatment
KW - Reverted austenite
UR - http://www.scopus.com/inward/record.url?scp=85110127961&partnerID=8YFLogxK
U2 - 10.1016/j.addma.2021.102176
DO - 10.1016/j.addma.2021.102176
M3 - Article
AN - SCOPUS:85110127961
SN - 2214-8604
VL - 46
JO - Additive Manufacturing
JF - Additive Manufacturing
M1 - 102176
ER -