Lead-free KNN-based thin films obtained by pulsed laser deposition

Brenda Carreño-Jiménez; Jose Luis Benitez-Benitez; Rosalba Castaneda-Guzman; M. Acuautla; Rigoberto Lopez-Juarez

doi:10.1109/ISAF51494.2022.9870118

Lead-free KNN-based thin films obtained by pulsed laser deposition

Brenda Carreño-Jiménez, Jose Luis Benitez-Benitez, Rosalba Castaneda-Guzman, M. Acuautla, Rigoberto Lopez-Juarez

Discrete Technology and Production Automation

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › Academic › peer-review

1 Citation (Scopus)

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Abstract

In this work, 0.96(K0.48Na0.52)0.95Li0.05Nb0.94Sb0.06O3−0.04Ba0.94Ca0.06ZrO3 (KNLNS-BCZ) and 0. 9S(K0.48Na0.52)0.95Li0.05Nb0.95Sb0.05O3−0.02Ba0.5(Bi0.5Na0.5)0.5ZrO3 (KNLNS-BBNZ) ferroelectric thin films were obtained by pulsed laser deposition. The structural, and morphological characteristics were studied to determine the best deposition parameters and analyse the piezoelectric properties. The studied deposition parameters were temperature, laser fluence, oxygen partial pressure and frequency. These parameters impact important characteristics of the thin films like grain morphology, thickness, and roughness. KNLNS-BCZ thin films with pure perovskite structure, homogeneous grain growth, and thickness ≥100 nm were fabricated at 700∘C,2J/cm2,300 mTorr, and frequencies of 5 Hz and 10 Hz. These films presented good ferroelectric behaviour and piezoelectric coefficient d 33eff of 83.80 pm/V and 25.80 pm/V, respectively.

Original language	English
Title of host publication	2022 IEEE International Symposium on Applications of Ferroelectrics, Piezoresponse Force Microscopy and European Conference on Applications of Polar Dielectrics, ISAF-PFM-ECAPD 2022
Place of Publication	Tours, France
Publisher	Institute of Electrical and Electronics Engineers Inc.
Number of pages	4
ISBN (Electronic)	9781665448413
DOIs	https://doi.org/10.1109/ISAF51494.2022.9870118
Publication status	Published - 2-Sept-2022
Event	2022 IEEE International Symposium on Applications of Ferroelectrics, ISAF 2022 - Tours, France Duration: 27-Jun-2022 → 1-Jul-2022

Conference

Conference	2022 IEEE International Symposium on Applications of Ferroelectrics, ISAF 2022
Country/Territory	France
City	Tours
Period	27/06/2022 → 01/07/2022

Keywords

and KNNbased.
Lead-free thin films
PLD method

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10.1109/ISAF51494.2022.9870118

Lead-free KNN-based thin films obtained by pulsed laser depositionFinal publisher's version, 3.03 MBLicence: Taverne

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Carreño-Jiménez, B., Benitez-Benitez, J. L., Castaneda-Guzman, R., Acuautla, M., & Lopez-Juarez, R. (2022). Lead-free KNN-based thin films obtained by pulsed laser deposition. In 2022 IEEE International Symposium on Applications of Ferroelectrics, Piezoresponse Force Microscopy and European Conference on Applications of Polar Dielectrics, ISAF-PFM-ECAPD 2022 Institute of Electrical and Electronics Engineers Inc.. https://doi.org/10.1109/ISAF51494.2022.9870118

Carreño-Jiménez, Brenda ; Benitez-Benitez, Jose Luis ; Castaneda-Guzman, Rosalba et al. / Lead-free KNN-based thin films obtained by pulsed laser deposition. 2022 IEEE International Symposium on Applications of Ferroelectrics, Piezoresponse Force Microscopy and European Conference on Applications of Polar Dielectrics, ISAF-PFM-ECAPD 2022. Tours, France : Institute of Electrical and Electronics Engineers Inc., 2022.

@inproceedings{fdff1db590654262bffd29ae40595306,

title = "Lead-free KNN-based thin films obtained by pulsed laser deposition",

abstract = "In this work, 0.96(K0.48Na0.52)0.95Li0.05Nb0.94Sb0.06O3−0.04Ba0.94Ca0.06ZrO3 (KNLNS-BCZ) and 0. 9S(K0.48Na0.52)0.95Li0.05Nb0.95Sb0.05O3−0.02Ba0.5(Bi0.5Na0.5)0.5ZrO3 (KNLNS-BBNZ) ferroelectric thin films were obtained by pulsed laser deposition. The structural, and morphological characteristics were studied to determine the best deposition parameters and analyse the piezoelectric properties. The studied deposition parameters were temperature, laser fluence, oxygen partial pressure and frequency. These parameters impact important characteristics of the thin films like grain morphology, thickness, and roughness. KNLNS-BCZ thin films with pure perovskite structure, homogeneous grain growth, and thickness ≥100 nm were fabricated at 700∘C,2J/cm2,300 mTorr, and frequencies of 5 Hz and 10 Hz. These films presented good ferroelectric behaviour and piezoelectric coefficient d 33eff of 83.80 pm/V and 25.80 pm/V, respectively.",

keywords = "and KNNbased., Lead-free thin films, PLD method",

author = "Brenda Carre{\~n}o-Jim{\'e}nez and Benitez-Benitez, {Jose Luis} and Rosalba Castaneda-Guzman and M. Acuautla and Rigoberto Lopez-Juarez",

note = "Funding Information: ACKNOWLEDGMENT Brenda Carre{\~n}o-Jim{\'e}nez gratefully thanks CONACyT-Mexico and University of Groningen for providing a PhD scholarship. Rigoberto Lop{\'e}z-Ju{\'a}rez thanks to DGAPA-UNAM for financial support under project number PAPIIT-IN113420. Rosalba Casta{\~n}eda-Guzm{\'a}n is acknowledged for the support to the projects PAPIIT IN104121 and CONACyT A1-S-22695. The authors want to acknowledge to Jos{\'e} Juan Gervacio Arciniega for the PFM analysis. Publisher Copyright: {\textcopyright} 2022 IEEE.; 2022 IEEE International Symposium on Applications of Ferroelectrics, ISAF 2022 ; Conference date: 27-06-2022 Through 01-07-2022",

year = "2022",

month = sep,

day = "2",

doi = "10.1109/ISAF51494.2022.9870118",

language = "English",

booktitle = "2022 IEEE International Symposium on Applications of Ferroelectrics, Piezoresponse Force Microscopy and European Conference on Applications of Polar Dielectrics, ISAF-PFM-ECAPD 2022",

publisher = "Institute of Electrical and Electronics Engineers Inc.",

}

Carreño-Jiménez, B, Benitez-Benitez, JL, Castaneda-Guzman, R, Acuautla, M & Lopez-Juarez, R 2022, Lead-free KNN-based thin films obtained by pulsed laser deposition. in 2022 IEEE International Symposium on Applications of Ferroelectrics, Piezoresponse Force Microscopy and European Conference on Applications of Polar Dielectrics, ISAF-PFM-ECAPD 2022. Institute of Electrical and Electronics Engineers Inc., Tours, France, 2022 IEEE International Symposium on Applications of Ferroelectrics, ISAF 2022, Tours, France, 27/06/2022. https://doi.org/10.1109/ISAF51494.2022.9870118

Lead-free KNN-based thin films obtained by pulsed laser deposition. / Carreño-Jiménez, Brenda; Benitez-Benitez, Jose Luis; Castaneda-Guzman, Rosalba et al.
2022 IEEE International Symposium on Applications of Ferroelectrics, Piezoresponse Force Microscopy and European Conference on Applications of Polar Dielectrics, ISAF-PFM-ECAPD 2022. Tours, France: Institute of Electrical and Electronics Engineers Inc., 2022.

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution › Academic › peer-review

TY - GEN

T1 - Lead-free KNN-based thin films obtained by pulsed laser deposition

AU - Carreño-Jiménez, Brenda

AU - Benitez-Benitez, Jose Luis

AU - Castaneda-Guzman, Rosalba

AU - Acuautla, M.

AU - Lopez-Juarez, Rigoberto

N1 - Funding Information: ACKNOWLEDGMENT Brenda Carreño-Jiménez gratefully thanks CONACyT-Mexico and University of Groningen for providing a PhD scholarship. Rigoberto Lopéz-Juárez thanks to DGAPA-UNAM for financial support under project number PAPIIT-IN113420. Rosalba Castañeda-Guzmán is acknowledged for the support to the projects PAPIIT IN104121 and CONACyT A1-S-22695. The authors want to acknowledge to José Juan Gervacio Arciniega for the PFM analysis. Publisher Copyright: © 2022 IEEE.

PY - 2022/9/2

Y1 - 2022/9/2

N2 - In this work, 0.96(K0.48Na0.52)0.95Li0.05Nb0.94Sb0.06O3−0.04Ba0.94Ca0.06ZrO3 (KNLNS-BCZ) and 0. 9S(K0.48Na0.52)0.95Li0.05Nb0.95Sb0.05O3−0.02Ba0.5(Bi0.5Na0.5)0.5ZrO3 (KNLNS-BBNZ) ferroelectric thin films were obtained by pulsed laser deposition. The structural, and morphological characteristics were studied to determine the best deposition parameters and analyse the piezoelectric properties. The studied deposition parameters were temperature, laser fluence, oxygen partial pressure and frequency. These parameters impact important characteristics of the thin films like grain morphology, thickness, and roughness. KNLNS-BCZ thin films with pure perovskite structure, homogeneous grain growth, and thickness ≥100 nm were fabricated at 700∘C,2J/cm2,300 mTorr, and frequencies of 5 Hz and 10 Hz. These films presented good ferroelectric behaviour and piezoelectric coefficient d 33eff of 83.80 pm/V and 25.80 pm/V, respectively.

AB - In this work, 0.96(K0.48Na0.52)0.95Li0.05Nb0.94Sb0.06O3−0.04Ba0.94Ca0.06ZrO3 (KNLNS-BCZ) and 0. 9S(K0.48Na0.52)0.95Li0.05Nb0.95Sb0.05O3−0.02Ba0.5(Bi0.5Na0.5)0.5ZrO3 (KNLNS-BBNZ) ferroelectric thin films were obtained by pulsed laser deposition. The structural, and morphological characteristics were studied to determine the best deposition parameters and analyse the piezoelectric properties. The studied deposition parameters were temperature, laser fluence, oxygen partial pressure and frequency. These parameters impact important characteristics of the thin films like grain morphology, thickness, and roughness. KNLNS-BCZ thin films with pure perovskite structure, homogeneous grain growth, and thickness ≥100 nm were fabricated at 700∘C,2J/cm2,300 mTorr, and frequencies of 5 Hz and 10 Hz. These films presented good ferroelectric behaviour and piezoelectric coefficient d 33eff of 83.80 pm/V and 25.80 pm/V, respectively.

KW - and KNNbased.

KW - Lead-free thin films

KW - PLD method

UR - http://www.scopus.com/inward/record.url?scp=85138724437&partnerID=8YFLogxK

U2 - 10.1109/ISAF51494.2022.9870118

DO - 10.1109/ISAF51494.2022.9870118

M3 - Conference contribution

AN - SCOPUS:85138724437

BT - 2022 IEEE International Symposium on Applications of Ferroelectrics, Piezoresponse Force Microscopy and European Conference on Applications of Polar Dielectrics, ISAF-PFM-ECAPD 2022

PB - Institute of Electrical and Electronics Engineers Inc.

CY - Tours, France

T2 - 2022 IEEE International Symposium on Applications of Ferroelectrics, ISAF 2022

Y2 - 27 June 2022 through 1 July 2022

ER -

Carreño-Jiménez B, Benitez-Benitez JL, Castaneda-Guzman R, Acuautla M, Lopez-Juarez R. Lead-free KNN-based thin films obtained by pulsed laser deposition. In 2022 IEEE International Symposium on Applications of Ferroelectrics, Piezoresponse Force Microscopy and European Conference on Applications of Polar Dielectrics, ISAF-PFM-ECAPD 2022. Tours, France: Institute of Electrical and Electronics Engineers Inc. 2022 doi: 10.1109/ISAF51494.2022.9870118

Lead-free KNN-based thin films obtained by pulsed laser deposition

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