Negative ion desorption chemical ionization mass spectrometry of some underivatized glucuronides

A. P. Bruins*

*Corresponding author for this work

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    Abstract

    Negative ion chemical ionization spectra, with [OH]− as the reactant ion are presented for some underivatized glucuronides R—O—gluc. The non‐volatile samples are introduced by thermal desorption from a Pt wire inside the source. The spectra show abundant [M—H]− ions, and [R—O]− ions, presenting information about the molecular weight and the aglycone. The method can be considered as an alternative to field desorption mass spectrometry, for characterization of compounds of these types.
    Original languageEnglish
    Pages (from-to)31-35
    Number of pages5
    JournalBiomedical mass spectrometry
    Volume8
    Issue number1
    DOIs
    Publication statusPublished - 1981

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