High-resolution and conventional electron microscopy study of a Sigma=3, [101]{121} twin grain boundary in molybdenum

T Vystavel*, JM Penisson, A Gemperle

*Corresponding author voor dit werk

OnderzoeksoutputAcademicpeer review

19 Citaten (Scopus)

Samenvatting

Complete structural analysis of a Mo bicrystal containing a Sigma =3, [101](1 (2) over bar1)(A) grain boundary (GB) was achieved by means of transmission electron microscopy from the microscopic to the nanoscopic level. Secondary GB dislocations compensating a small deviation from the exact Sigma =3 concidence were observed and their character was determined. Rigid-body displacements (RBDs) were determined directly from high-resolution electron microscopy images using samples with surface normal parallel and perpendicular to the tilt axis. Measured values of RBDs are compared with recent theoretical calculations.

Originele taal-2English
Pagina's (van-tot)417-429
Aantal pagina's13
TijdschriftPhilosophical Magazine A-Physics of Condensed Matter Structure Defects and Mechanical Properties
Volume81
Nummer van het tijdschrift2
StatusPublished - feb.-2001

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