Samenvatting
Complete structural analysis of a Mo bicrystal containing a Sigma =3, [101](1 (2) over bar1)(A) grain boundary (GB) was achieved by means of transmission electron microscopy from the microscopic to the nanoscopic level. Secondary GB dislocations compensating a small deviation from the exact Sigma =3 concidence were observed and their character was determined. Rigid-body displacements (RBDs) were determined directly from high-resolution electron microscopy images using samples with surface normal parallel and perpendicular to the tilt axis. Measured values of RBDs are compared with recent theoretical calculations.
Originele taal-2 | English |
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Pagina's (van-tot) | 417-429 |
Aantal pagina's | 13 |
Tijdschrift | Philosophical Magazine A-Physics of Condensed Matter Structure Defects and Mechanical Properties |
Volume | 81 |
Nummer van het tijdschrift | 2 |
Status | Published - feb.-2001 |